反应详情

温度

65 °C

To a 30 mL vial containing a stirring bar DMSO-D6 (0.5 mL), pyridine-D5 (1 drop), 3-trifluoromethylphenylisocyanate (14 mg, 0.080 mol) and 2-Phosphono-4-bromoaniline disodium salt (10 mg, 0.036 mmol) were added. The resulting mixture was stirred at 65° C. for 3 hours, resulting in a DMSO solution of the desired urea.

1. additionwere added