HCID 21930284, compound → HCID 21930293, compound

HRID 1243660Notes

Reaction equation

HRID 1243660 reaction equation
[Cl:1]CC([NH:5][CH2:6][C:7]1[CH:12]=[C:11](OC(F)(F)F)[CH:10]=[CH:9][C:8]=1[O:18][CH3:19])=O.ClCC(NCC1C=CC(OC(F)(F)[F:34])=CC=1O)=O>>[ClH:1].[F:34][C:11]1[CH:10]=[CH:9][C:8]([O:18][CH3:19])=[C:7]([CH:12]=1)[CH2:6][NH2:5]

Participants

3

Reactant 2

HCID 21930284HCID 21930284, compoundHCID 21930302HCID 21930302, compound

Product 1

HCID 21930293HCID 21930293, compound

Procedure

This compound was prepared using the procedure described in Example 74, using 2-chloro-N-(2-methoxy-5-trifluoromethoxy-benzyl)-acetamide, instead of 2-chloro-N-(2-hydroxy-4-trifluoromethoxy-benzyl)-acetamide. 1H NMR (CD3OD) δ=7.15–7.11 (2H, m), 7.06–7.03 (1H, m), 4.06 (2H, s), 3.88 (3H, s).

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-9304edea3b1947728b6f425b3d8b7086
Source dataset
uspto-grants-2006_10
Patent number
US07119120B2

Reaction notes

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