3,5-Di-tert-butyl-4-hydroxybenzoic acid → HCID 178440952, compound

HRID 1244490Notes

Reaction equation

HRID 1244490 reaction equation
[ClH:1].CC(C1C=C(C=C(C(C)(C)C)C=1O)[C:9]([N:11]1[CH2:16][CH2:15][N:14]([C:17]2[CH:22]=[CH:21][C:20]([NH:23][C:24]([C:26]3[S:27][CH:28]=[CH:29][CH:30]=3)=[NH:25])=[CH:19][CH:18]=2)[CH2:13][CH2:12]1)=[O:10])(C)C.[C:39]([C:43]1[CH:44]=[C:45]([CH2:54]C(O)=O)[CH:46]=[C:47]([C:50]([CH3:53])([CH3:52])[CH3:51])[C:48]=1[OH:49])([CH3:42])([CH3:41])[CH3:40].C(C1C=C(C=C(C(C)(C)C)C=1O)C(O)=O)(C)(C)C>>[ClH:1].[CH3:42][C:39]([C:43]1[CH:44]=[C:45]([CH2:54][C:9]([N:11]2[CH2:12][CH2:13][N:14]([C:17]3[CH:22]=[CH:21][C:20]([NH:23][C:24]([C:26]4[S:27][CH:28]=[CH:29][CH:30]=4)=[NH:25])=[CH:19][CH:18]=3)[CH2:15][CH2:16]2)=[O:10])[CH:46]=[C:47]([C:50]([CH3:53])([CH3:52])[CH3:51])[C:48]=1[OH:49])([CH3:40])[CH3:41]

Participants

4

Reactant 3

HCID 150073,5-Di-tert-butyl-4-hydroxybenzoic acidHCID 27751103,5-Bis(1,1-dimethylethyl)-4-hydroxybenzeneacetic acidHCID 178441075HCID 178441075, compound

Product 1

HCID 178440952HCID 178440952, compound

Procedure

The experimental protocol used is the same as that described for the compound 9, with 3,5-di-tert-butyl-4-hydroxyphenylacetic acid replacing the 3,5-di-tert-butyl4-hydroxybenzoic acid in the first stage of synthesis. Yellow powder. Melting point: 176-180° C.

Workup

  1. customin the first stage of synthesis

Sources & evidence

ORD record
ord-a7dec8dcf6e94e33b731008454df43a0
Source dataset
uspto-grants-2006_10
Patent number
US07122535B2

Reaction notes

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