Methanesulfonyl chloride → HCID 69104534, compound

HRID 1244543Notes

Reaction equation

HRID 1244543 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]([N:12]2[CH2:16]CC[CH2:13]2)=[NH:11])=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH3:17][S:18](Cl)(=[O:20])=[O:19]>>[CH3:13][N:12]([CH3:16])[C:10](=[N:11][S:18]([CH3:17])(=[O:20])=[O:19])[C:7]1[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 21919785HCID 21919785, compound

Product 1

HCID 69104534HCID 69104534, compound

Procedure

Part B: According to the procedure described Example 57, part C, 1.14 g (5.9 mmol) of (4-nitrophenyl)(pyrrolidin-1-yl)methanimine were reacted with methane sulfonyl chloride to yield N,N-dimethyl-N′-(methylsulfonyl)-4-nitrobenzamidine (890 mg).

Sources & evidence

ORD record
ord-a4957f2cf7084fc2abaa35e7c4cb5b72
Source dataset
uspto-grants-2006_10
Patent number
US07122557B2

Reaction notes

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