Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Itaconic acid | HCID 811 | — |
| Reactant | 4-Benzyloxyaniline | HCID 22860 | — |
| Product | STK087815 | HCID 2968114 | 96.2% |
Reaction Steps
18.8 g (94.4 mmol) 4-benzyloxyaniline are mixed with 12.28 g (94.4 mmol) itaconic acid. The mixture is heated to 130° C. After 20 min the melted material solidifies. The resulting solid is triturated with ethyl acetate to yield 28.26 g (96%) of a greyish solid. MS: m/e=311 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07122562B2 |
|---|
| Source dataset | uspto-grants-2006_10 |
|---|
| ORD ID | ord-2efdc15ea29a44e8a10338f1448071d0 |
|---|
| Source note | uspto-grants-2006_10 |
|---|
