Glyoxal → 4-[1,2,4]Triazolo[4,3-b][1,2,4]triazin-3-ylmethyl-phenol

HRID 1244638Notes

Reaction equation

HRID 1244638 reaction equation
[CH:1](=O)[CH:2]=O.[NH2:5][N:6]1[C:10]([NH2:11])=[N:9][N:8]=[C:7]1[CH2:12][C:13]1[CH:18]=[CH:17][C:16]([OH:19])=[CH:15][CH:14]=1>>[N:9]1[N:8]=[C:7]([CH2:12][C:13]2[CH:18]=[CH:17][C:16]([OH:19])=[CH:15][CH:14]=2)[N:6]2[C:10]=1[N:11]=[CH:2][CH:1]=[N:5]2

Participants

3

Reactant 2

HCID 7860GlyoxalHCID 219193134-[(4,5-Diamino-4H-1,2,4-triazol-3-yl)methyl]phenol

Product 1

HCID 113107094-[1,2,4]Triazolo[4,3-b][1,2,4]triazin-3-ylmethyl-phenol

Procedure

General procedure A was followed with the reaction of ethanedial and 4-(4,5-diamino-4H-[1,2,4]triazol-3-ylmethyl)-phenol to provide 4-[1,2,4]triazolo[4,3-b][1,2,4]triazin-3-ylmethyl-phenol (example 7).

Sources & evidence

ORD record
ord-3beca4c1183342caab11ca99238d99e6
Source dataset
uspto-grants-2006_10
Patent number
US07122548B2

Reaction notes

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