4-Fluorobenzaldehyde → HCID 69123797, compound

HRID 1244662Notes

Reaction equation

HRID 1244662 reaction equation
[F:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.Cl.[S:11]([C:15]1[CH:20]=[CH:19][C:18]([NH:21][NH2:22])=[CH:17][CH:16]=1)(=[O:14])(=[O:13])[NH2:12]>>[S:11]([C:15]1[CH:16]=[CH:17][C:18]([NH:21][N:22]=[CH:6][C:5]2[CH:8]=[CH:9][C:2]([F:1])=[CH:3][CH:4]=2)=[CH:19][CH:20]=1)(=[O:14])(=[O:13])[NH2:12]

Participants

3

Reactant 2

HCID 680234-FluorobenzaldehydeHCID 27945674-Hydrazinylbenzenesulfonamide hydrochloride

Product 1

HCID 69123797HCID 69123797, compoundYield 58%

Procedure

A solution of 4-fluorobenzaldehyde (5 mmol) and 4-sulfamyl-phenylhydrazine hydrochloride was subjected to the General Procedure. The title compound, melting point 205–206° C., was obtained in 58% yield.

Sources & evidence

ORD record
ord-d9458cf112be4f638c023406c84ee828
Source dataset
uspto-grants-2006_10
Patent number
US07122571B2

Reaction notes

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