Methacrylic Acid → HCID 9878948, compound

HRID 1244864Notes

Reaction equation

HRID 1244864 reaction equation
C(O[Si:5]([CH2:14][CH2:15][CH2:16][CH3:17])([CH2:10][CH2:11][CH2:12][CH3:13])[CH2:6][CH2:7][CH2:8][CH3:9])(=O)C.[C:18]([OH:23])(=[O:22])[C:19]([CH3:21])=[CH2:20]>>[C:18]([O:23][Si:5]([CH2:10][CH2:11][CH2:12][CH3:13])([CH2:14][CH2:15][CH2:16][CH3:17])[CH2:6][CH2:7][CH2:8][CH3:9])(=[O:22])[C:19]([CH3:21])=[CH2:20]

Participants

3

Reactant 2

HCID 4093Methacrylic AcidHCID 21923874HCID 21923874, compound

Product 1

HCID 9878948HCID 9878948, compound

Procedure

4 g of acetoxytri-n-butylsilane and 1.33 g of commercial methacrylic acid (ATOFINA Norsocryl® MAA) are mixed at room temperature, acetic acid is then distilled under reduced pressure (45° C./13 hPa) to afford tri-n-butylsilyl methacrylate.

Workup

  1. distillationacetic acid is then distilled under reduced pressure (45° C./13 hPa)

Sources & evidence

ORD record
ord-b81975780a8f473fbf6f0842cd3ca3f1
Source dataset
uspto-grants-2006_10
Patent number
US07122692B2

Reaction notes

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