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HRID1244882

反应详情

EQUATION

反应方程式

HRID 1244882 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccccc1I
HCID10784

2-Iodophenol

C6H5IO

2 次

结构：CC1(C)OB(c2ccccc2)OC1(C)C
HCID570673

4,4,5,5-Tetramethyl-2-phenyl-1,3,2-dioxaborolane

C12H17BO2

PRODUCTS

生成物

1
结构：CC1(C)OB(c2cccc(O)c2)OC1(C)C
HCID2734623

3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

C12H17BO3

PROCEDURE

实验过程

The above reaction procedure used for 2-iodophenol was followed. The reaction was faster, being complete before the first sample for gc analysis was withdrawn after 1 h 50 min reaction time. The amount of phenylboronic acid pinacol ester was higher than in the 2-iodophenol reaction (around 7%).

WORKUP

后处理

  1. customThe above reaction procedure
  2. customwas withdrawn after 1 h 50 min
  3. customreaction time