HCID 21923033, compound → HCID 178478740, compound

HRID 1244955Notes

Reaction equation

HRID 1244955 reaction equation
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4]([NH:16][CH2:17][CH2:18][NH:19][C:20](=[O:29])[C:21]2[CH:26]=[C:25]([Cl:27])[CH:24]=[C:23]([Cl:28])[CH:22]=2)[N:3]=1.[NH2:30][C@H:31]1[CH2:36][CH2:35][C@H:34]([NH2:37])[CH2:33][CH2:32]1>>[ClH:1].[ClH:1].[NH2:30][C@H:31]1[CH2:36][CH2:35][C@H:34]([NH:37][C:2]2[N:10]=[C:9]3[C:5]([N:6]=[CH:7][N:8]3[CH:11]3[CH2:15][CH2:14][CH2:13][CH2:12]3)=[C:4]([NH:16][CH2:17][CH2:18][NH:19][C:20](=[O:29])[C:21]3[CH:22]=[C:23]([Cl:28])[CH:24]=[C:25]([Cl:27])[CH:26]=3)[N:3]=2)[CH2:33][CH2:32]1

Participants

3

Reactant 2

HCID 21923033HCID 21923033, compoundHCID 178511674HCID 178511674, compound

Product 1

HCID 178478740HCID 178478740, compound

Conditions

Temperature
140 °C

Procedure

360 mg of the product obtained in Stage 1 above and 450 mg of trans-1,4-diaminocyclohexane are mixed together and the reaction medium is heated to approximately 140° C. for 6 hours.

Sources & evidence

ORD record
ord-b19ba985ba554391a9ad6982b834510e
Source dataset
uspto-grants-2006_10
Patent number
US07122669B1

Reaction notes

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