HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57457971, compound → HCID 57457960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57457971 | HCID 57457971 | — |
| Reactant | HCID 57501866 | HCID 57501866 | — |
| Product | HCID 57457960 | HCID 57457960 | 36% |
Reaction Steps
In a similar manner to the procedures described in Preparative Examples 12(v)′, 12(vi)′ and 12(vii)′ above, reactions were conducted in turn, using (S)-1-benzyloxycarbonyl-4,4-dimethyl-2-hydroxymethylpyrrolidine [obtained as described in Preparative Example 17(i)′ above] instead of (2S,4S)-1-benzyloxycarbonyl-2-hydroxymethyl-4-methylthiopyrrolidine, to give the title compound as a brown oil (yield: 36%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122666B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-189580c743a54085b3feab641bfbd26d |
| Source note | uspto-grants-2006_10 |