HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-1-Benzyl 2-methyl 4-methylenepyrrolidine-1,2-dicarboxylate → HCID 57457961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-1-Benzyl 2-methyl 4-methylenepyrrolidine-1,2-dicarboxylate | HCID 54190049 | — |
| Reactant | HCID 69558769 | HCID 69558769 | — |
| Product | HCID 57457961 | HCID 57457961 | 10% |
Reaction Steps
In a similar manner to the procedures described in. Preparative Examples 8(ii)′, 8(iii)′, 8(iv)′, 8(v)′ and 8(vi)′ above, reactions were conducted in turn, using (S)-1-benzyloxycarbonyl-4-ethylideneproline methyl ester [prepared as described in Preparative Example 24′ above] instead of (S)-1-benzyloxycarbonyl-4-methylideneproline methyl ester, to give the title compound as a brown oil (yield: 10%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122666B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-754e786f52404ff8aec0b97b636cad3f |
| Source note | uspto-grants-2006_10 |