HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21921667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Iodoheptane | HCID 20274 | — |
| Reactant | Methyl 5-bromosalicylate | HCID 77683 | — |
| Product | HCID 21921667 | HCID 21921667 | — |
Reaction Steps
5-Bromo-2-heptyloxy-benzoic acid was prepared by reacting 5-bromo-2-hydroxy-benzoic acid methyl ester (1.0 g, 4.32 mmol) with iodoheptane (1.46 g, 6.49 mmol) as per general procedure H with potassium carbonate (1.5 g, 10.8 mmol) added. The ester thus obtained was subjected to hydrolysis as per general procedure C to yield the 5-Bromo-2-heptyloxy-benzoic acid (0.950 gm, 70%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122580B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-4d6b0648d17d40b8a08da8b21b0dcc09 |
| Source note | uspto-grants-2006_10 |