HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21919204, compound → HCID 21919135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21919204 | HCID 21919204 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21919135 | HCID 21919135 | 81% |
Reaction Steps
Methyl 3-(3,4,5,6-tetramethoxy-2-methylbenzyl)-2-benzyloxybenzoate (343 mg, 0.7360 mmol) was dissolved in methanol (10 ml), added to a methanolic suspension (40 ml) of 10% palladium-carbon (100 mg) and stirred for 16 hours at room temperature in a hydrogen atmosphere. The reaction solution was filtered and the filtrate was concentrated under reduced pressure to give the title compound (223 mg, 0.5930 mmol, 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07122543B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-9fd49105a7574f4ab900332f7cd524db |
| Source note | uspto-grants-2006_10 |