HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → 3-Chloro-N-(4-ethyl-5-methyl-1,3-thiazol-2-yl)-2-methylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 4-Ethyl-5-methyl-1,3-thiazol-2-amine | HCID 3164022 | — |
| Product | 3-Chloro-N-(4-ethyl-5-methyl-1,3-thiazol-2-yl)-2-methylbenzenesulfonamide | HCID 9923601 | 12% |
Reaction Steps
The title compound was prepared from 4-ethyl-5-methyl-1,3-thiazol-2-ylamine (METHOD I) and 3-chloro-2-methylbenzenesulfonyl chloride according to METHOD A, yellowish foam, 40 mg (12% yield): HRMS Calcd (found) for C13H15ClN2O2S2 m/z 330.0263 (330.0271).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125900B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-961f8344607a4c57ad038b2b79d97588 |
| Source note | uspto-grants-2006_10 |