Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4-Dichloro-6-methylbenzenesulfonyl chloride → Ethyl 3-(2-{[(2,4-dichloro-6-methylphenyl)sulfonyl]amino}-1,3-thiazol-4-yl)-3-methylbutanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| 반응물 | HCID 21914681 | HCID 21914681 | — |
| 생성물 | Ethyl 3-(2-{[(2,4-dichloro-6-methylphenyl)sulfonyl]amino}-1,3-thiazol-4-yl)-3-methylbutanoate | HCID 10225906 | — |
반응 단계
The title compound was prepared from ethyl 3-(2-amino-1,3-thiazol-4-yl)-3-methylbutanoate (METHOD I) and 2,4-dichloro-6-methylbenzenesulfonyl chloride as described in the synthetic method to give a white solid (55.0 mg) with purity >90%. MS (pos) m/z 451.2, 453.2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07125900B2 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-88f5b3c88e4b45a3b4c8e2de5a494adf |
| 출처 메모 | uspto-grants-2006_10 |