HRID1245651
反应详情
EQUATION
反应方程式
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反应物
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生成物
PROCEDURE
实验过程
The title compound was prepared from 5-acetyl-2-amino-4-methylthiazole (42 mg) and 2,4,5-trichlorobenzenesulfonyl chloride (76 mg) as described in the synthetic METHOD B to give a white solid (23.7 mg) with purity >90%: MS (pos) m/z 399.2, 401.2; HRMS m/z 397.9103 (calc. of monoisotopic mass for C12H9Cl3N2O3S2 gives 397.9120).