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HRID1245709

反应详情

EQUATION

反应方程式

HRID 1245709 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OI1(OC(C)=O)(OC(C)=O)OC(=O)c2ccccc21
HCID159087

Triacetoxyperiodinane

C13H13IO8

结构：CCC(CO)Nc1cc(C)nc(Oc2c(C)cc(Cl)cc2C)c1C(=O)OC
HCID10178647

未命名化合物

PRODUCTS

生成物

1
结构：CCC(C=O)Nc1cc(C)nc(Oc2c(C)cc(Cl)cc2C)c1C(=O)OC
HCID86584329

未命名化合物

PROCEDURE

实验过程

The title compound was prepared by Dess-Martin oxidation of 2-(4-chloro-2,6-dimethyl-phenoxy)4-(1-hydroxymethyl-propylamino)-6-methyl-nicotinic acid methyl ester. The title compound was obtained after column chromatography. 1H NMR (CDCl3) 9.54(d,1H), 8.56(d,1H), 7.01(s,2H), 5.93(s,1H), 3.92(m,1H), 3.89(s,3H), 2.08(s,3H), 2.05(s,6H), 1.05(t,3H) ppm.