Water → HCID 21914366, compound

Participants

Reaction Conditions

Reaction Steps

Potassium carbonate (9.12 g) was suspended in dimethylformamide (25 ml) and 2-bromophenol (3.46 g) was added portionwise. Benzyl bromide (3.76 g) was added and the mixture heated to 60° C. for 4 h. After cooling the mixture was added to water (250 ml) and extracted three times with diethyl ether. The organic layer was separated and washed with 2M sodium hydroxide solution (100 ml) before drying over sodium sulphate. After filtration, evaporation yielded (5.13 g) as a colourless oil.

Provenance & Evidence