HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21914252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Piperidine, 1-(2-chloroethyl)-, hydrochloride | HCID 74826 | — |
| Reactant | HCID 21914298 | HCID 21914298 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21914252 | HCID 21914252 | 106.6% |
Reaction Steps
4-Bromo-3-hydroxyphenyl 4-methylbenzenesulfonate (17.6 g), potassium carbonate (7.32 g), 1-(2 chloroethyl)piperidine hydrochloride (9.2 g) and acetone (300 ml) were stirred at reflux for 3 h, the reaction mixture filtered and evaporated to give the product as light brown foam (24.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07125896B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-8edf2da733ad44cd94869e3315c0a7bd |
| Source note | uspto-grants-2006_10 |