2-Bromophenol → HCID 21914441, compound

HRID 1245869Notes

Reaction equation

HRID 1245869 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[OH:8].CS(O[CH:14]1[CH2:18][CH2:17][N:16]([CH3:19])[CH2:15]1)(=O)=O>>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[O:8][CH:14]1[CH2:18][CH2:17][N:16]([CH3:19])[CH2:15]1

Participants

3

Reactant 2

HCID 72442-BromophenolHCID 219142741-Methylpyrrolidin-3-yl methanesulfonate

Product 1

HCID 21914441HCID 21914441, compound

Procedure

The title compound was prepared from 2-bromophenol and 1-methylpyrrolidin-3-yl methanesulphonate in a similar manner to Example 134 (b) except that the compound was purified by cation exchange chromatography eluting with ammonia/methanol mixtures.

Workup

  1. customwas purified by cation exchange chromatography
  2. washeluting with ammonia/methanol mixtures

Sources & evidence

ORD record
ord-73f1c1e377404723813d31857df5d581
Source dataset
uspto-grants-2006_10
Patent number
US07125896B2

Reaction notes

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