Dabsyl chloride → n-{2-[2-(4-Amino-2,6,7-trimethyl-1h-imidazo[4,5-c]pyridin-1-yl)ethoxy]ethyl}-4-{[4-(dimethylamino)phenyl]diazenyl}benzenesulfonamide

Participants

Role	Name	HCID	Charge
Reactant	Dabsyl chloride	HCID 91660	—
Reactant	1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine	HCID 21913053	—
Product	n-{2-[2-(4-Amino-2,6,7-trimethyl-1h-imidazo[4,5-c]pyridin-1-yl)ethoxy]ethyl}-4-{[4-(dimethylamino)phenyl]diazenyl}benzenesulfonamide	HCID 10437562	—

Reaction Steps

Using the method of Examples 34–50, 4-dimethylaminoazobenzene-4′-sulfonyl chloride was reacted with 1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The product was purified using Method A. The observed accurate mass was 551.2551.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07125890B2
Source dataset	uspto-grants-2006_10
ORD ID	ord-ec34b1a2c33544819adc8c4538e5cc77
Source note	uspto-grants-2006_10