HRID1246576

反应详情

EQUATION

反应方程式

HRID 1246576 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Silver Sulfamerazine was prepared using 26.43 g sulfamerazine, 300 ml of water, 4.00 grams of NaOH warming to 70 degree C. until dissolved. 16.99 grams of silver nitrate in 300 grams of water with 1 drop of 10% nitric acid and warming to 70 degree C. The sulfamerazine solution was added to the silver nitrate solution with stirring. Silver sulfamerazine precipitated as a fine white powder. This was filtered and washed three times with water and dried overnight at 60 deg to give an off-white powder.

WORKUP

后处理

  1. customto 70 degree
  2. dissolutionuntil dissolved
  3. customSilver sulfamerazine precipitated as a fine white powder
  4. filtrationThis was filtered
  5. washwashed three times with water
  6. customdried overnight at 60 deg
  7. customto give an off-white powder