HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → Codeinone 14-Hydroxycodeinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | (4R,4aS,12bS)-4a-hydroxy-9-methoxy-3-methyl-2,4,7a,13-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-7-one | HCID 5359420 | — |
| Reactant | Codeinone | HCID 5459910 | — |
| Product | Codeinone 14-Hydroxycodeinone | HCID 131726012 | — |
Reaction Steps
25±1 mg of both codeinone and 14-hydroxycodeinone reference materials were weighed and transferred into a 100-mL volumetric flask, diluted to volume and dissolved with ˜0.85% phosphoric acid solution II.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07129248B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-2557194413894cafa19c812493ebd905 |
| Source note | uspto-grants-2006_10 |