HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2-Fluoro-5-nitrobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-Fluoro-5-nitrobenzoic acid | HCID 280997 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | Methyl 2-Fluoro-5-nitrobenzoate | HCID 11217860 | 99% |
Reaction Steps
A solution of 2-fluoro-5-nitrobenzoic acid (200 mg, 1.08 mmol) in 0.7 M HCl in methanol was stirred for 5 h. The mixture was concentrated yielding 210 mg (99%) of the title compound; which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07129245B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-c7d4c2dbcf48436db6e4a9d5d85de090 |
| Source note | uspto-grants-2006_10 |