HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloropyridine-2-carboxylic acid → HCID 21906537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloropyridine-2-carboxylic acid | HCID 230890 | — |
| Reactant | HCID 21906567 | HCID 21906567 | — |
| Product | HCID 21906537 | HCID 21906537 | 82.5% |
Reaction Steps
Using a similar procedure to that described in Example 52, N-(5-chloropyridin-2-yl)-5-methoxycarbonyl-2-[(4-piperidinylmethyl)amino]benzamide (0.30 g, 0.74 mmol) and 4-chloropicolinic acid (0.23 g, 1.5 mmol) afforded 320 mg (82%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07129245B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-f0166ccaab2e4101a3fdfe428a49edf9 |
| Source note | uspto-grants-2006_10 |