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Methyl 2-Bromo-5-nitrobenzoate → Methyl 2-(2'-formylphenyl)-5-nitrobenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 2-Bromo-5-nitrobenzoate | HCID 245494 | — |
| 反応物 | 2-Formylphenylboronic acid | HCID 292189 | — |
| 生成物 | Methyl 2-(2'-formylphenyl)-5-nitrobenzoate | HCID 21907645 | — |
反応手順
Methyl 2-bromo-5-nitrobenzoate was coupled to 2-formylphenylboronic acid using the procedure described for Example 4, Part A to provide methyl 2-(2′-formylphenyl)-5-nitrobenzoate. 1HNMR (300 MHz, CDCl3) δ 8.91 (s, 1H); 8.42 (d, 1H, J=8.5 Hz); 8.00 (d, 1H, J=8.5 Hz); 7.64 (m, 2H); 7.47 d, 1H, J=8.5 Hz); 7.22 (d, 1H, J=8.5 Hz); 3.71 (s, 3H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07129264B2 |
| 出典データセット | uspto-grants-2006_10 |
| ORD ID | ord-35a88fcf307c4b61878dbd41bc97e8fd |
| 出典メモ | uspto-grants-2006_10 |