1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one → HCID 13475995, compound

HRID 1247961Notes

Reaction equation

HRID 1247961 reaction equation
[NH2:1][C:2]1[C:6]([C:7]([C:9]2[S:10][CH:11]=[CH:12][N:13]=2)=[O:8])=[CH:5][NH:4][N:3]=1.CN(C)[CH:16]=[CH:17][C:18]([C:20]1[CH:21]=[N:22][CH:23]=[CH:24][CH:25]=1)=O>>[N:22]1[CH:23]=[CH:24][CH:25]=[C:20]([C:18]2[N:3]3[N:4]=[CH:5][C:6]([C:7]([C:9]4[S:10][CH:11]=[CH:12][N:13]=4)=[O:8])=[C:2]3[N:1]=[CH:16][CH:17]=2)[CH:21]=1

Participants

3

Reactant 2

HCID 5670331-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-oneHCID 178509270HCID 178509270, compound

Product 1

HCID 13475995HCID 13475995, compound

Procedure

As described for Example 1, (3-amino-1H-pyrazol-4-yl)-2-thiazolyl-methanone was reacted with 3-dimethylamino-1-(3-pyridinyl)-2-propen-1-one to give the product as colorless crystals, mp 262°-264° C.

Sources & evidence

ORD record
ord-b33b92da086d4d049b8ac4824c8bf537
Source dataset
uspto-grants-1985_06
Patent number
US04521422

Reaction notes

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