Zincchloride → HCID 20263423, compound

Participants

Reaction Steps

A mixture is prepared by admixing 7.9 g of the sodium salt of 3,4-dimethylpyrazole-1-carbodithioate in 50 ml of deionized water. This mixture is added to a mixture of 2.6 g of zinc chloride in 250 ml of deionized water. A precipitate formed immediately and the product was recovered by filtration and dried. The product was recovered in a yield of 6.2 g (75 percent of theoretical). The product decomposed above 210° C. Upon analysis, the product was found to have carbon, hydrogen and nitrogen contents of 36.88, 3.54 and 14.31 percent, respectively, as compared with the theoretical contents of 37.10, 3.63 and 14.42 percent, respectively, as calculated for the above-named compound.

Provenance & Evidence