HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 13476556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 13476555 | HCID 13476555 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13476556 | HCID 13476556 | — |
Reaction Steps
1.2 g of 1-[2-(cyclohexylmethyl)-n-hexyl]imidazole, as an oil, was dissolved in ether (50 ml). Sulfuric acid was added dropwise until precipitation was complete. The hydrogen sulfate salt was collected and recrystallized from ethyl acetate to give 1-[2-cyclohexylmethyl-n-hexyl]imidazole hydrogen sulfate, m.p. 152° C. (gels), 190°-192° C. final melt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04522948 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-86ce9cd33b004f28b91953f4a8a9c81f |
| Source note | uspto-grants-1985_06 |