HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorobenzoyl chloride → HCID 178496933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorobenzoyl chloride | HCID 66645 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 5-Methoxybenzocyclobutene-1-carboxylic acid methyl ester | HCID 54118413 | — |
| Product | HCID 178496933 | HCID 178496933 | — |
Reaction Steps
In a manner analogous to that described in Example 5, starting from 26.6 g of aluminium trichloride, 9.61 g of 5-methoxybenzocyclobutene-1-carboxylic acid methyl ester and 20.95 g of 2,4-dichlorobenzoyl chloride there is obtained 4-(2,4-dichlorobenzoyl)-5-hydroxybenzocyclobutene-1-carboxylic acid methyl ester having a melting point of 99°-100°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04523030 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-fbea0220bd6b49d5837f15bd072fe64a |
| Source note | uspto-grants-1985_06 |