HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Hydroxyacetophenone → HCID 178465686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Hydroxyacetophenone | HCID 7469 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | Hydroxylamine, sulfate (1:1) | HCID 159255 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178465686 | HCID 178465686 | 173.7% |
Reaction Steps
A solution was prepared by adding 20.4 g (0.15 mol) of 4-hydroxyacetophenone and 13.0 g (0.08 mol) of hydroxylamine sulfate to 100 mL of water at 70° C. To the solution was added 16.3 mL of 30% ammonium hydroxide which was then heated at reflux for 0.5 h. White crystals formed upon cooling yielding 21.0 g (92.6%) of 4-hydroxyacetophenone oxime.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04524217 |
| Source dataset | uspto-grants-1985_06 |
| ORD ID | ord-cfe4534417504ca9ae295af9bb2a7d4d |
| Source note | uspto-grants-1985_06 |