HCID 86741136, compound → HCID 86741135, compound

HRID 1248803Notes

Reaction equation

HRID 1248803 reaction equation
C[N:2]([CH3:20])[CH:3]=[CH:4][C:5]([C:7]1[CH:8]=[C:9]([CH2:13][CH2:14][NH:15][C:16](=[O:19])[O:17][CH3:18])[CH:10]=[CH:11][CH:12]=1)=O.N[C:22]1[C:26]([C:27]#[N:28])=C[NH:24][N:23]=1>>[C:27]([C:26]1[CH:22]=[N:23][N:24]2[C:5]([C:7]3[CH:8]=[C:9]([CH2:13][CH2:14][NH:15][C:16](=[O:19])[O:17][CH3:18])[CH:10]=[CH:11][CH:12]=3)=[CH:4][CH:3]=[N:2][C:20]=12)#[N:28]

Participants

3

Reactant 2

HCID 86741136HCID 86741136, compoundHCID 178510443HCID 178510443, compound

Product 1

HCID 86741135HCID 86741135, compound

Procedure

A 2.76 g portion of [3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]ethylcarbamic acid, methyl ester was reacted with 1.08 g of 3-aminopyrazole-4-carbonitrile as described in Example 13, giving 2.6 g of the desired product, mp 162°-164° C.

Sources & evidence

ORD record
ord-d80b011ea86a4f89b6429309e2152599
Source dataset
uspto-grants-1986_12
Patent number
US04626538

Reaction notes

Loading…