HCID 86741138, compound → HCID 86741137, compound

HRID 1248804Notes

Reaction equation

HRID 1248804 reaction equation
C[N:2]([CH3:21])[CH:3]=[CH:4][C:5]([C:7]1[CH:8]=[C:9]([CH2:13][CH2:14][NH:15][C:16](=[O:20])[O:17][CH2:18][CH3:19])[CH:10]=[CH:11][CH:12]=1)=O.N[C:23]1[C:27]([C:28]#[N:29])=C[NH:25][N:24]=1>>[C:28]([C:27]1[CH:23]=[N:24][N:25]2[C:5]([C:7]3[CH:8]=[C:9]([CH2:13][CH2:14][NH:15][C:16](=[O:20])[O:17][CH2:18][CH3:19])[CH:10]=[CH:11][CH:12]=3)=[CH:4][CH:3]=[N:2][C:21]=12)#[N:29]

Participants

3

Reactant 2

HCID 86741138HCID 86741138, compoundHCID 178510443HCID 178510443, compound

Product 1

HCID 86741137HCID 86741137, compound

Procedure

A 2.0 g portion of [3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]ethylcarbamic acid, ethyl ester was reacted with 1.08 g of 3-aminopyrazole-4-carbonitrile as described in Example 13, giving 2.52 g of the desired product, mp 133°-135° C.

Sources & evidence

ORD record
ord-4f46ac0297f14fb48aa9d1e18cc5d84f
Source dataset
uspto-grants-1986_12
Patent number
US04626538

Reaction notes

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