HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → N-[3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]-N-2-propenylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | N-[3-(3-Dimethylaminoacryloyl)phenyl]acetamide | HCID 53412415 | — |
| Product | N-[3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]-N-2-propenylacetamide | HCID 54234186 | — |
Reaction Steps
An 11.61 g portion of N-[3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]acetamide was reacted with 7.26 g of allyl bromide as described in Example 6, giving 13.34 g of N-[3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]-N-2-propenylacetamide, mp 91°-94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04626538 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-165c699154f14b5497f9e8fdc03f8adc |
| Source note | uspto-grants-1986_12 |