HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propyne, 1-bromo- → N-[3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]-N-2-propynylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propyne, 1-bromo- | HCID 137279 | — |
| Reactant | N-[3-(3-Dimethylaminoacryloyl)phenyl]acetamide | HCID 53412415 | — |
| Product | N-[3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]-N-2-propynylacetamide | HCID 54294873 | — |
Reaction Steps
An 11.61 g portion of N-[3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]acetamide was reacted with propynyl bromide as described in Example 6, giving N-[3-[3-(dimethylamino)-1-oxo-2-propenyl]phenyl]-N-2-propynylacetamide, mp 98°-101° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04626538 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-c3b756cad6a7484d9f75f639218059cb |
| Source note | uspto-grants-1986_12 |