Butanal → HCID 20226086, compound

HRID 1248819Notes

Reaction equation

HRID 1248819 reaction equation
[C:1]([O:5][C:6]([NH:8][C:9]1[S:13][N:12]=[C:11]([CH2:14][C:15]([O:17][CH2:18][CH3:19])=[O:16])[N:10]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH:20](=[O:24])[CH2:21][CH2:22][CH3:23]>>[C:1]([O:5][C:6]([NH:8][C:9]1[S:13][N:12]=[C:11]([CH:14]([CH:20]([OH:24])[CH2:21][CH2:22][CH3:23])[C:15]([O:17][CH2:18][CH3:19])=[O:16])[N:10]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 261ButanalHCID 20226075HCID 20226075, compound

Product 1

HCID 20226086HCID 20226086, compound

Procedure

1.0 g (3.5 mMol) of product from Example 28 were reacted with 0.9 ml (~10 mMol) of n-butanal for 5 days in the manner described in Example 29 and then purified by chromatography on silica gel. Yield 0.17 g (14% of theory).

Workup

  1. custompurified by chromatography on silica gel

Sources & evidence

ORD record
ord-b5f3c17004ba4878b7760c8d67487afa
Source dataset
uspto-grants-1986_12
Patent number
US04626535

Reaction notes

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