Heptanal → HCID 20226083, compound

HRID 1248822Notes

Reaction equation

[C:1]([O:5][C:6]([NH:8][C:9]1[S:13][N:12]=[C:11]([CH2:14][C:15]([O:17][CH2:18][CH3:19])=[O:16])[N:10]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH:20](=[O:27])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[C:1]([O:5][C:6]([NH:8][C:9]1[S:13][N:12]=[C:11]([CH:14]([C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH:20]([OH:27])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[N:10]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 8130Heptanal

HCID 20226075HCID 20226075, compound

Product 1

HCID 20226083HCID 20226083, compound

Procedure

1.0 g (3.5 mMol) of product from Example 28 were reacted with 1.46 ml (~10 mMol) of n-heptanal in the manner described in Example 29. Yield of erythro/threo mixture of the title compound: 1.4 g.

Sources & evidence

ORD record: ord-cd77e8cb16ea4db79782d8ff0bc18492
Source dataset: uspto-grants-1986_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04626535

Reaction notes

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