HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-2-(Acetoxyacetyl)-1-(tert-butoxycarbonyl)pyrrolidine → 2(s)-(Acetoxyacetyl)-pyrrolidine trifluoroacetic acid salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-2-(Acetoxyacetyl)-1-(tert-butoxycarbonyl)pyrrolidine | HCID 13753435 | — |
| Reactant | Trifluoroacetic acid acetate | HCID 23437676 | — |
| Product | 2(s)-(Acetoxyacetyl)-pyrrolidine trifluoroacetic acid salt | HCID 13753439 | — |
Reaction Steps
A solution of 1.00 g of the product of Example 2 can be kept in 10 ml of 1:1 trifluoracetic acid-acetic acid at 20° for 30 minutes. The solvents can then be removed under reduced pressure to give (S)-2-(2-acetoxy-1-oxoethyl)-pyrrolidine trifluoracetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04626545 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-7fa09c580400450d840324a66d338ebb |
| Source note | uspto-grants-1986_12 |