HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Bromoacetamido-3-(2,6-dichlorobenzoylamino)methylceph-3-em-4-carboxylic acid → 7-(1,2,3,4-Thiatriazole-5-ylthio)-acetamido-3-(2,6-dichlorobenzoylamino)methylceph-3-em-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Bromoacetamido-3-(2,6-dichlorobenzoylamino)methylceph-3-em-4-carboxylic acid | HCID 14502350 | — |
| Reactant | HCID 178527995 | HCID 178527995 | — |
| Product | 7-(1,2,3,4-Thiatriazole-5-ylthio)-acetamido-3-(2,6-dichlorobenzoylamino)methylceph-3-em-4-carboxylic acid | HCID 131714986 | 65% |
Reaction Steps
1.0 g. of 7-bromoacetamido-3-(2,6-dichlorobenzoylamino)methylceph-3-em-4-carboxylic acid and 0.24 g. of 5-mercapto-1,2,3,4-thiatriazole were reacted and worked up according to the method of Example 15. Thus 0.73 g. (65%) of 7-(1,2,3,4-thiatriazole-5-ylthio)-acetamido-3-(2,6-dichlorobenzoylamino)methylceph-3-em-4-carboxylic acid were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04626533 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-556aab5d7c9f4d5f90e2b8f00f5c9e27 |
| Source note | uspto-grants-1986_12 |