HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioanisole → Methyl phenyl sulfoxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioanisole | HCID 7520 | — |
| Reactant | Sodium Hypochlorite | HCID 23665760 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Methyl phenyl sulfoxide | HCID 14516 | — |
Reaction Steps
To a solution of methyl-phenyl-sulphide (6.2 g) in water (2 ml) and dioxane (98 ml), stirred at 20° C. (external bath), sodium hypochlorite (88.69 g, titre 4.19%, pH 12.5) is added in 30 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628087 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-e313766bb7b74f65a9dde9c55327884b |
| Source note | uspto-grants-1986_12 |