HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13753877, compound → HCID 13753878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13753877 | HCID 13753877 | — |
| Catalyst | Manganese oxide | HCID 160959 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13753878 | HCID 13753878 | 73% |
Reaction Steps
To 2.07 g of 1-[2-hydroxy-4-[(6-hydroxy-4-hexynyl)oxy]-3-propylphenyl]ethanone in 150 ml of methylene chloride at 25° was added 20.7 g of activated manganese oxide and the mixture was stirred for 2 hours. After filtration, the filtrate was concentrated in vacuo to yield 1.50 g (73% yield) of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628115 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-d087d8e85264426c990d2c88f220f5f4 |
| Source note | uspto-grants-1986_12 |