HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13561927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Allyl chloride | HCID 7850 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1,2,3,4-Tetrahydro-Beta-Carboline-3-Carboxylic Acid | HCID 98285 | — |
| Product | HCID 13561927 | HCID 13561927 | 59% |
Reaction Steps
In the same manner as described in Example 6, (3RS)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (3.24 g), KOH (1.75 g), 50% ethanol (60 ml), carbon disulfide (1.8 ml) and allyl chloride (2.3 g) are reacted and treated. The product is crystallized from chloroform to give the title compound (3.0 g, 59%), m.p. 161°-162° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628057 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-c3b6bc3173b04ecd8826998e2c2a399a |
| Source note | uspto-grants-1986_12 |