反应详情

In the same manner as descsribed in Example 32, (3RS)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (4.32 g), 20N NaOH (2.2 ml), carbon disulfide (1.45 ml), dimethylsulfoxide (13 ml) and 2-thenyl chloride (3.18 g) are reacted and treated. The product is crystallized from ethanol to give the title compound (4.1 g) as pale yellow crystals, m.p. 172° C. (decomp.).

1. customare reacted
2. additiontreated
3. customThe product is crystallized from ethanol