HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 13561953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Furfuryl Alcohol | HCID 7361 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(Chloromethyl)furan | HCID 219520 | — |
| Reactant | D-1,2,3,4-Tetrahydronorharman-3-carboxylic acid | HCID 675102 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 13561953 | HCID 13561953 | — |
Reaction Steps
In the same manner as descsribed in Example 32, (3R)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (8.65 g), KOH (4.67 g), carbon disulfide (2.43 ml), 75% ethanol (120 ml) and furfuryl chloride which is prepared from furfuryl alcohol (9.24 g), thionyl chloride (12.34 g) and pyridine (8.94 g) are reacted and treated to give the title compound (2.31 g) as pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628057 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-4d04b1f0650b4fee9de48418bb2f4bae |
| Source note | uspto-grants-1986_12 |