HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 53996224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Bromomethylstyrene | HCID 98116 | — |
| Reactant | 1,2,3,4-Tetrahydro-Beta-Carboline-3-Carboxylic Acid | HCID 98285 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 53996224 | HCID 53996224 | 32.8% |
Reaction Steps
In the same manner as descsribed in Example 32, (3RS)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (2.16 g), 10N NaOH (2 ml), carbon disulfide (912 mg), dimethylsulfoxide (6 ml) and cinnamyl bromide (2.364 g) are reacted and treated. The product is crystallized from ethanol to give the title compound (1.34 g), m.p. 200°-202° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628057 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-b9cac1cb557d4b20b37e49c87db1805e |
| Source note | uspto-grants-1986_12 |