HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 1769752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 40535462 | HCID 40535462 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 1769752 | HCID 1769752 | 79.4% |
Reaction Steps
In the same manner as described in Reference Example 2-(1) using methyl (1RS,3SR)-trans-1-butyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylate (2.0 g), 1N NaOH (8.2 ml) and methanol (35 ml), there is obtained the title compound (1.51 g, 79%) as colorless needles, m.p. 204°-205° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04628057 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-0164e3404c224331a3f51a833f275aa4 |
| Source note | uspto-grants-1986_12 |