HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1249240Generated: November 1, 2026
Sodium borohydride → HCID 21284013, compound
https://huagongshe.com/reaction/1249240
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 21284015 | HCID 21284015 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 21284013 | HCID 21284013 | — |
Reaction Steps
1.5g Methyl 2-(4-bromo-3-oxobutanamido)acetate is dissolved in 15 ml dimethoxyethane. The solution is cooled to 0° C. and 60 mg NaBH4 is added. After 5 min, the solvent is evaporated in vacuo and the residue is chromatographed on silica, eluting with ethyl acetate. The title compound is obtained as a white powder, m.p. 60°-61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04629797 |
|---|
| Source dataset | uspto-grants-1986_12 |
|---|
| ORD ID | ord-2891037a489749278ef37cf5410830bc |
|---|
| Source note | uspto-grants-1986_12 |
|---|
