HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl pyruvate → HCID 86741160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl pyruvate | HCID 11748 | — |
| Reactant | Boc-Lys(Z)-OH | HCID 2724765 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86741160 | HCID 86741160 | — |
Reaction Steps
Dissolve 7.6 g Nα -Boc-Nε -Cbz-L-lysine and 2.04 g methyl pyruvate in 75 ml methanol. Add 2 g 10% palladium on charcoal and hydrogenate at an initial pressure of 40 psig for 3 hours at room temperature. Filter the solution and concentrate the filtrate at aspirator pressure to obtain Nα -Boc-Nε -(1-methoxycarbonylethyl)-L-lysine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04629787 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-add10bd86f084d29bce5b1b6cb171718 |
| Source note | uspto-grants-1986_12 |