HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium cyanoborohydride → HCID 18605797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 11543093 | HCID 11543093 | — |
| Reactant | HCID 18605799 | HCID 18605799 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 18605797 | HCID 18605797 | — |
Reaction Steps
React 1.08 g 3-(S)-amino-1-carboxymethylperhydroazepin-2-one hydrochloride, 5.3 g ethyl 2-oxo-5-phenylpentanoate, 0.49 g triethylamine and 630 mg sodium cyanoborohydride as described in Example 2. Purify the crude product by chromatography on LH 20 and isolate the desired ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04629787 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-916b8f1f8eae465da028b3602a398acd |
| Source note | uspto-grants-1986_12 |